| CAD4 |
 |
21 May 2010
Conditions
-
The Service Manual is written for service man with experience, so can sometimes
be too compressed for customers. It is also less cared for then a Technical
User Manual.
-
The use of this manual is for responsibility of the customer. If you are
not sure: ask Service and we will point out which part can be used.
-
Bruker AXS cannot give free technical assistance for problems, caused by
using this manual or other use which is not connected to a specific error.
Start-up or communication
error
-
Check the fuse at the back of the
interface.
-
Be sure no residual CAD4 programs are running
in the background as a result of a non standard previous exit.
-
Be sure to use the best start-up:
-
First start the program till it waits with the output : ".... Connection
is made to CAD4 process ....."
-
Power-up the interface
-
Check the 5V power during starting
up, when a high current is running.
-
Be sure there is no collision during start-up. Check it by putting an isolator
(piece of paper) between the collision switches.
-
Errors during porgram startup:
-
If the programs ends with: unit 3 = ......
-
Check if the GCU unit (if present) power is on
-
"Return Code 0": this means that the program is aborting itself (normally
with Ctrl-Y): probably an unreliable PC.
-
Check the RS232 indicator on front of the Interface (or with older CAD4
: mount a RS232 indicator between the CC connector and RS232 cable) and
check
-
After start-up the TXD should flash once. If not :
-
After TXD the RXD should flash. If not then there is a problem with the
computer
-
Check the Computer program
-
Try another RS232 port of the computer
-
TXD and RXD flash and the computer program runs till "CAD4H" (PC-DOS or
Digital)
-
Check the Bus interface 0546.604/614/554
-
Check with a digital probe the RS232 signal trough IC32 and return trough
IC33 (HCPL 2531) or replace both at once.
-
Check in the pocket terminal if the text "CAD4H" is running. When it stands
still or is absent, the program is dead.
-
The problem can now be in any part of the electronic, such as the processor.
Send the interface to the factory for repair.
Positioning errors
-
No motors are running :
-
Check the motor power supply in the Substitution unit (LED's on the outside).
-
General
-
Change in GONCON, CASPAR: PA = 10 (checks on a
larger positioning error). When the goniometer runs all right this setting
can be used temporary till the next maintenance service visit.
-
On the pocket terminal press: arrow, 7, move, axis and when it runs
press: 0. Now the axis should stop. If it runs the motor board is defect.
-
Interchange both motor boards and check if the problem is now in the other
axis. If it is then the error is in a board.
-
Oscillation (noise in the motor) :
-
If on a fixed position: probably an encoder problem.
-
Check the motor constants with GONCON, CASPAR, O with the factory values
on the paper in the accessories box.
-
Omega:
-
One of both motors defect: Remove the motor wires and turn them by hand.
It should run very smooth.
-
Check bearings: are they worn or rusty?
-
Check the gears: is there dirt or much backlash?
-
It could even be the column, but that is difficult to check
-
Axis running full speed in one direction
-
Remove the Motor Generator board
-
if still running at full speed the error is in a Motor drive board in FR58..
or Substitution unit.
-
if not running then probably the opto isolator
on the Motor Generator board is defect.
-
All axes 3 degree wrong position:
-
Phi and Kappa :
-
Check if there is a defect in the cable running trough the centre of the
goniometer:
-
Rotate Omega and check in the pocket terminal if Phi or Kappa position
change. If it does, the wires to the encoder are broken
-
Run Phi or Kappa (arrow 6) and rotate Omega by hand (by opening the plate
on the readout dials). Check if the motor runs smoothly. If not then the
wires to the motor are broken
-
If case of an error: change the cable.
-
Theta (sticks) :
-
Remove the side plate of the Omega indicator. Rotate the indicator by hand.
When it is not running smoothly, probably the column is defect, perhaps
caused by overflowing with nitrogen.
-
Remove the side plate of the Theta indicator. Rotate the indicator by hand.
When it is not running smoothly, probably the course encoder is defect.
When it sticks every 2.8º it is the fine encoder. If it sticks on
one position : the coarse encoder. The mechanics must be dismantled to
check where is the error.
-
Does it stops once at low speed? Sometimes the dial counter has a heavy
switch-over point. When it does not repeat it is no problem.
-
Remove the dial at the side of the goniometer, which can run heavy. It
is not essential for measurements.
-
Stops often: with Turbo-CAD4: motor worn. Open the motor at the back and
check if the collimators are worn.
-
Omega
-
Does it stops once at low speed? Sometimes the dial counter has a heavy
switch-over point. When it does not repeat it is no problem.
-
Remove the dial at the side of the goniometer, which can run heavy. It
is not essential for measurements.
-
Stops often: with Turbo-CAD4: motor worn. Open the motor at the back and
check if the collimators are worn.
-
Other: run on the pockterminal the
TEST
ALL.
211
13212
5413
44042
24071
626655
52362222220000000000000000305075 |
Coarse: Coarse encoder not at zero. Can cause the axis at 2.8º
wronmg position. Erro is very rare, mostly when some one has changed something
on the encoder.
Solve by: rezero |
-
-
Slits positioning problem:
-
Never change the dial position relative to the encoder, because realign
can only be done in the factory.
-
Positioning always has a tolerance of several bits, because it has backlash
to let the mechanical click determine the exact position.
-
Remove the cap of the dial unit and inspect the mechanical click.
-
Check if the ball of the spring is still present
-
Position the slit both from right and from left and check if the dial always
falls in the slit position.
-
Never change the position of the spring, unless you are sure the position
does not change. Realign the dial unit can only be done in the factory.
-
Check if the motor has an active stop :
-
On pocket terminal press : arrow, 6, move, dial. The dial will now rotate.
-
Press : 0. The dial should now stop immediately
-
Check on broken wires :
-
On pocket terminal press : spec, dial. This will show the dial position.
-
Rotate Theta and check if the dial position does not change.
-
Set the slit positive and negative with Theta on maximum positions and
check if the dial positions are all right.
Crash
-
Running out of crash:
-
Electronic
-
Stop all operations (when working with the pocket terminal : CLEAR).
-
Check which axis must be moved to recover from crash position and in which
direction.
-
In pocket terminal press : > 3 MOVE axis CRASH. (> or < depending
on direction : > = positive, < = negative). The goniometer will now
move a small step. Check if it moves in the right direction. Repeatedly
pressing CRASH moves the goniometer out of the crash switch, then
it will move continuously.
-
Stop movement with CLEAR.
-
Mechanical
-
Remove the side plate of the Omega or Theta dial and move it by hand out
of crash.
-
Crash message without real crash.
-
Now and then crasH
-
Check if the crash switches (at both collimators) is not to sensitive.
This can be done by slightly pushing or slide piec of paper in teh switch
(only temporary!) and check if the crashes disappear.
-
It can be caused by electronic spikes on the crash line. Place a capacitor
of 1 uF on the Motor Generator board between IC11
pin 1 ("LIMSW") and TP18 (GND).
-
Check the voltage between the metal parts of the collision switch (see
circuit)
-
If +12V then the opto IC11 on the Motor
generator board is defect
-
If 0V then remove the Motor generator board and measure again:
-
If +12V then opto IC11 is defect
-
If 0V then there is still a real short circuit in the crash circuit.
Crystal axis too long or too
short
-
Check with command WO if the right X-ray tube is selected.
Shutter does not open
-
The red shutter lamp goes on (temporary) but the shutter does not open.
This error is mostly caused by a safety error. Check in which part is the
error:
-
Shift the collimator backwards as far as possible with the right pin position.
-
Override the enclosure safety by connecting the flashing lamp to the Enclosure
connector (goniometer connector 1).
Be sure the lamp is flashing. If the shutter now opens, check if all the
doors are closed.
-
Place new lamps in the red shutter on lamp.
-
When you have recently (re)mounted the monochromator or X-ray port : Loosen
the two screw of the monochromator/X-ray port, press it to the collimator
holder and fasten the screws again.
-
Below the collimator holder there are two connections with a red and blue
wire (the collimator safety). Short circuit them and check if the shutter
opens. If so: inform Service. For safety : never
use this short circuit permanent.
HT falls off when using the
shutter
The shutter does not close fast enough so the safety electronics detects
an open shutter while it should be closed. It is indicated by a red computer
led on the FR586 or shutter message on the FR590. A service men must readjust
the shutter or probably replace the shutter coil. It is possible to remain
working temporary by opening the shutter with the pocket terminal before
the measurement, so it will be open continuously. Because
the shutter is always open this is only allowed when all safeties are active,
like the enclosure safety. The beam open lamp must not flash.
Attenuator does not
work
-
Set the attenuator and rotate the Theta axis. When the attenuator comes
in now and then, the wire in the Theta cable is broken. The cable must
be replaced by a servicemen.
Intensity problems
-
No intensity:
-
Check all fuses at the Interface backside
-
Measure the HV at the coax cable at the detector side it should be about
the same as the pocket terminal HV value.
-
If not present:
-
Check if the HV connector is mounted in the right connector at the interface
-
Probably the Power board defect.
-
Set the generator to 25 kV, 5 mA. Attenuator on, aperture to 9 mm, Theta
= 0, pin hole in collimator place, remove beam stop and measure the primary
beam. Give the result to the Service.
-
Intensity too low:
-
Be sure there is no obstruction anywhere in the X-ray path: attenuator
up, no slit in place (open hole).
-
Measure the intensity with Effic
-
Readjust the HV
-
Mount a new X-ray tube
-
Realign the X-ray optics
Program stops
after HV-off
-
With rotating anode:
-
Check in GONCON • CASPAR if it is set as rotating anode.
-
There is a difference in program:
-
Unix (Argus) and DOS : If HV does not return within 1.5 minute, the program
is stopped, asking if it should proceed.
-
EXPRESS is always starting trough.
Cannot find (strong) reflections
during Search
Intensities skipped:
copied previous data
When for some reason a reflection could not be measured, the data of
previous reflection is put into the log file.
-
Check the code if it shows a reason of not measuring
Program error messages. see
paper User Manual chapter VI-G, page 19. Small selection:
-
"collision": predicted collision
-
"crash-switch detected": real collision
-
"fading #me/#ref <<err": The data collection is interrupted
because an intensity-control reflection has become too weak. #me = as measured,
#ref = expected, err = max difference
-
Check the generator setting
-
Check the alignment of the crystal
-
"hard interrupt": defect Encoder board (micro-processor)
-
"noise": Intensity too low, reflection reset to "no valid information"
-
"not found": The reflection is not found and its line is deleted
form the Crystal file
-
"positoning time-out error": The data collection is interrupted
because the goniometer could not be positioned properlyu within 10 minutes.
See
above
-
"strong": intensity was above 50 kcps
-
"switch xxx1": The program was intterrupted by the user with a switch
xxx1 set. To continue it is necessary to reset this switch
-
"user interrupt": Program stopped by Ctrl-C or Ctrl-S from the host
computer.
-
"weak": Intensity too low, reflection reset to "no valid information"
Computer problems
-
Digital (VAX)
-
Does not boot, ends with >>>> prompt
-
Type command: SHOW BOOT.
-
The computer will search for a boot disk. If he finds one then command:
BOOT device name
-
If he does not find one then the disk is defect. Unless you can find an
old second hand part or repair shop the computer is not useful anymore.
-
New Linux or Express program does not run : Check upgrade
-
After command Zero or View, the message: HARD INTERRUPT
-
Collision switch activated
-
Respond with : /
Shutter circuit overview
HV-on circuit overview
Motor/encoder mechanical
overview
Crash/collision circuit
Potmeter test, TEST ALL
This test checks the servo system, mostly the behaviour of the encoder
potmeters.
-
Connect a printer or terminal to the RS232 CT port. at the backside of
the Interface. see specifications
-
Start the test on the pocket terminal with: • , move, 5 (or other
option).
-
Output :
| Theta |
Phi |
Fine test.
Measures during running the difference between wanted and real position
of the fine potmeter in digitization bits |
| Omega |
Kappa |
| Theta |
Phi |
Coarse test
Measures during running the difference between the 5 overlap bits of
the fine and course potmeter (positioning errors will exist with overflows,
so with errors larger then 15 columns). |
| Omega |
Kappa |
- Limits : width <14 columns and not two peaks. Mostly
the fine test will show an error.
- The left bit is all overflows (+ and -)
- Other errors |
Examples
Phi coarse: Zero shifted. See Adjust
33
32111
015
06340
656
725067
73342222200000000000000000000530751
Motor encoder board
To change opto couplers (type HP 2531). When changing it is advised
it mount them on a IC socket
Register
-
Read out the status register with the pocket terminal: 174124 MOVE
0 (Motor generator board IC29)
-
Normal output with X-ray on and shutter closed: CA 177760
-
CA 177761 = X-ray off (bit D0 = 1)
-
CA 177762 = Shutter switch indicates an open shutter (bit D1 = 1)
-
CA 177770 = Collision detected (bit D3 = 1)
| Software commands
(selection) |
Program and general
| VAX |
PC-DOS |
Linux |
|
| CAD4 #L |
CAD4 #L |
CAD4 #L |
Start CAD4 program # (mostly 0) L = forced loading |
| EXIT, QUIT |
EXIT |
EXITXX |
Exit program in the normal way |
| Ctrl-C, Ctrl-C |
CTR-Y |
Ctrl-Z |
Abort program |
SHOW SYS
STOP ID#### |
not needed |
kill %
abort_cad4 # |
Remove residual programs after abort (### = pid number of CAD* programs) |
| Q |
|
|
With inputs: quit command |
| / |
|
|
With inputs: default |
| @name |
|
|
Starts a command file name.DAT in [CAD4.DATAn] |
| LOG |
|
|
Makes a new log file in [CAD4.DATAn], default : CD4CA4.LOG |
CAPRT, E
CAPRT, D |
|
|
Output to terminal / printer serial line (CT port)
enabled or disabled |
| CONSW |
|
|
Switches to in/output on terminal serial line (CT
port) (or back to host computer when used on terminal) |
|
|
|
|
Crystal file
| GONCON, FCRYST, Y, name, Y, Q, LK, 1, 25 |
Makes a new crystal file with max. 25 reflections (then do SEARCH).
See User manual page 9/2 |
| LO #1 #2 |
Shows the list of reflections from reflection #1 to #2. Output :
n - h - k - l - * - Theta - Phi - **s - attenuator/speed - width (3*FWHM
in º) - counts |
| LH, h k l |
Adds a reflection to the list (then do SETANG to measure) |
| LK, #1 #2 |
Removes reflections #1 to #2 from the list. |
| LCA, #, A, Y |
Sets a reflection "unmeasured" (then do SETANG to measure). |
| RO |
Displays : data and orientation of the crystal. |
| WO |
Displays : X-ray tube, Lam1 and Lam2 (wavelength of alpha1 and alpha2,
depending on X-ray tube) and attenuator filter factor. |
| WI |
For input the : X-ray tube (Mo, Cu, Ag, Cr, Co, Fe) and attenuator
filter factor. |
|
|
Measure, position
| SETANG |
Measures the "unmeasured" reflections in the list. Output :
n - * - Theta/K - S - Phi/K - Omega/K - Kappa/K - Phi/E - Omega/E -
Chie/E - Shifts..... |
|
| SCAN, axes, SA, N, R |
Scan axes ( = P, T, O, K). SA = angle (º), N = speed (º/min
= N/16.48), R = ratio of two axes (1-6). |
|
| SCAN, N, time |
Intensity / time measurement without moving axes (multiple measurements).
Switch = 0001 : only one measurement. |
|
| SEARCH, T K P, SP DV |
Search new reflections for the empty places in the crystal file.
See SEARCH
T C P = Phi scan on position Theta and Chie.
SP = Scan speed 1 - 12 (x16.48 º/min).
DF = Discrimination factor peak/background. |
|
| SETPAR, swoma swomb diafra diafrb scanr qfact pfract |
Scan parameters. See Measure crystal
swoma, swomb = the omega scan is swoma + swomb * tan(Theta)
diafra, diafrb = the aperture is diafra + diafrb * tan(Theta)
scanr = scan ratio
qfact = Quality factor
pfract = Poisson distribution factor
Output : SETPAR with input / / / / / /. |
|
LG, n, .P
KP, Theta Phi Omega Kappa
EP, Theta Phi Omega Chie
MK
ME |
Position goniometer axes
Output : position |
on reflex n
in Kappa
in Eulerian
in Kappa
in Eulerian |
| SAP, n |
Position of the aperture. Default : 9 mm / open hole. n = mm |
|
SP
SN
SH
SV |
Position to slit |
positive skew
negative skew
horizontal
vertical |
SA
RA |
Attenuator |
in
out |
SO
SC |
Shutter |
Open
Close |
|
|
|
|
|
|
Standard output of a
measurement (paper User Manual chapter XI-E, page 29)
Type 0
|
type |
list nr
1-25 |
H |
K |
L |
code |
Theta
º |
Phi-K
º |
Omega-K
º |
Kappa
º |
NPI = Scan speed
16.48/NPI º/min
- = with attenuator |
Scan width |
Netto intensity |
| default example: |
1 |
|
-3 |
-1 |
12 |
N***** |
|
|
|
|
3 |
|
|
Type 1
|
type |
reflection
number |
H |
K |
L |
code |
Psi |
Npi = Scan speed
16.48/Npi º/min
- = with attenuator |
Background intensity
left
sum profile 1-16 |
Intensity
sum profile 17-80
type 3 |
background intensity
right
som profile 81-96 |
? |
? |
| number of characters: |
2 |
6 |
5 |
5 |
5 |
7 |
7 |
4 |
6 |
7 |
6 |
|
|
| default example: |
1 |
1450 |
-3 |
-1 |
12 |
N***** |
.00 |
3 |
14 |
2424 |
8 |
793.3 |
16.7 |
Type 2
|
type |
reflection
number |
Theta
º |
Phi-K
º |
Omega-K
º |
Kappa
º |
Width Omega scan
º |
Cumulative X-ray time
s |
Fridl |
| number of characters: |
2 |
6 |
8 |
9 |
9 |
9 |
7 |
7 |
3 |
| default example: |
2 |
1450 |
|
|
|
|
|
|
|
Typ 3-10
|
type |
reflection
number |
96 dumps of intensities of the scan
columns with intensity vertical in cnt |
| default example: |
2 |
1450 |
3211133
06340015
725067656
00000000005307517334222220000000000 |
Code reflection status (see paper User Manual,
chapter XI-E, page 30)
-
N***** = normal
-
I***** = intensity control
-
N**W** = weak reflection
-
N**S** = strong reflection
-
N**T** = too strong reflection, even with attenuator
-
NC**** = predicted collision
-
ND**** = Shift oif the reflection more then DANG
-
NX**** = Chie > 100º, so no positioning possible
Express
It is also possible to work with the basic (old) CAD4 program:
-
Build a stand-alone CAD4:
-
Command: @expressgen cad4
-
Do everything asked for after the above command
-
Copy: [express.system]accesscode.exp to: [cad4.system]
-
SET DEF [CAD4.SYSTEM]
-
@CAD4 0
Express commands and keys functions:
| EXP 0 |
Startup Express |
| EXIT |
Normal exit |
| 3x Ctrl-C |
Abort |
| LOG/CAD4/NEW filename |
Makes a new CAD4 log-file. Default: [EXPRESS.DATA#]CD4XB#.LOG |
|
|
| Keys: |
|
| PF1 |
Cancel. Exit subwindow: |
| PF2 |
Help |
| PF3 |
Select expanded window |
| - |
Erase window |
| , |
Toggle window |
| . |
Temporary to VMS. Return with EXP 0 |
| enter |
Cancel/confirm goniometer errors |
| 1-8 |
Window position |
| 5 |
Errors window |
| ctrl-R |
Rewrite screen |
| ctrl-B |
Abort goniometer command |
|
|
|
|
|
|
|
|
Pocket terminal, normal use
|
|
|
SL4
SR4 |
Shifts 32 character data in the 8 character window (use when
you have "lost" the data). After start-up : always 5 times SL4 to get the
right readout position. |
|
ABS
REL |
Display the intensity absolute (ABS) or relative to the first
measurement in percentage steps (REL). |
|
| +xx.xx MOVE axis |
Moves axis to position +xx.xxº |
|
| > n MOVE axis |
Rotate axis with speed n (1-9) in positive (>) or negative (<)
direction. Pressing another speed number or (< n) or (> n) during rotation
immediately changes the speed or direction. |
|
| > 3 MOVE axis CRASH |
Position after a crash |
|
| SWITCH |
Switch register. To change : xxxx MOVE SWITCH
0001 = goniometer stops after the current movement
0000 = repeats movements
Extra output on the CAD4 CT port (not the host),
see User manual page 6/13-17:
2000 = Profiles of centring routine , 4000 = Measured reflection, 0400
= Search data |
|
CLEAR
MOVE, CLEAR
SPEC, CLEAR
PAUSE |
Stop |
All functions
Move functions
Input and display
Till pause is pressed again. |
Pocket terminal, service
use
|
|
|
SPEC, axis
SPEC, MOVE, axis |
Encoder position (potmeter) of the chosen axis. Output in octal
value
- Choice : C/F = coarse/fine, D/S = Cosine/Sine
- Default after clear : course and cosine |
Coarse and fine. Choose C/F
Potmeter. Choose C/F and D/S |
•, MOVE, 5
–, MOVE, 5
SPEC, axis, degree, MOVE, 5 |
Potmeter (servo) test, course and
fine. |
Course and fine
Only course
Over degree of axis from present position |
| address, MOVE, 0 |
Data read |
|
| HV, LL, WD |
Detector HV voltage, Lower Level and Window.
xxx MOVE HV. Change HV. this will not be saved in GONCON !
> n MOVE HV/LL/WD Scans HV, LL or WD with speed n. |
|
| xxx MOVE PAUSE |
Set CAD4 CT port (not the host !) to xxxx baud
. This is not saved in GONCON! |
|
|
|
|
Program error messages
-
see paper User Manual chapter VI-G, page 19
-
"hard interrupt": defect Encoder board (micro-processor)
Program error messages
| COLLIS |
Predicted collision |
| CO RUNS |
Tried to operate the goniometer by pocket terminal while Host computer
is running a goniometer action (it was under target microprocessor control
) |
| CRASH |
The goniometer is in a crash position |
| INP ERR |
The entered input is not valid |
|
|
For testing, use the test crystal.
Measuring a crystal
Scan parameters setting with SETPAR.
-
Default :
-
With Mo :
-
Default : SETPAR, 0.80 0.35 2.40 1.05 6. 1.00 1.00
-
Sharp or strong reflection : SETPAR, 0.45 0.35 1.90 1.05 6. 0.60 2.50
-
With Cu :
-
Default : SETPAR, 0.80 0.15 2.40 0.43 6. 1.00 1.00
-
Sharp or strong reflection : SETPAR, 1.20 0.15 3.00 0.43 6. 2.00 0.70
Search
-
Look in the crystal list with LO.
-
If it is empty :
-
Command SEARCH, [T] 0 90, 12 2
-
If it is not empty (also when it is from another crystal) :
-
Remove reflections 1-3 (LK, 1 3) and : SEARCH, [T] 0 90, 12 2
-
Remove reflections 4-6 (LK, 4 6) and : SEARCH, [T] 15 90, 12 2
-
Remove reflections 7-9 (LK, 7 9) and : SEARCH, [T] 30 90, 12 2
-
Remove reflections 10-12 (LK, 10 12) and : SEARCH, [T] 45 90, 12 2
-
This will search reflections at different positions, which will index more
quickly.
-
[T] = 7 for Mo and 15 for Cu
-
When it cannot find a reflection, try another
setting
Connections,
fuses, boards
-
1 : 4 pin, Radiation safety shield (safety switches) or safety override
flashing lamp.
-
2 : 6 pin, Optional Kappa Limit safety switch. When not used, a
dummy connector must be mounted.
-
3 : 2 pin, Crystal illumination (24V, max. 80 mA)
-
4 : 7 pin, to the Pocket terminal (adapter).
-
5 : "G" cable to the FR586 or Substitution unit.
-
6 : "M" cable to the Goniometer Interface.
-
M : "M" cable, to the goniometer
-
R : "R" cable, to the 586 or Substitution unit
-
CT : RS232 connection for an extra console terminal
or printer.
-
CC : RS232 connection to the Host computer.
-
When using a PC with 9 pin connector: buy a standard RS232 0-modem cable
or connect as:
| 25 pin |
9 pin |
| pin 2 |
pin 2 |
| pin 3 |
pin 3 |
| pin 7 |
pin 5 |
| pin 4 to pin 5 and pin 8 |
pin 1 to pin 7 and pin 8 |
| pin 6 to pin 20 |
pin 4 to pin 6 |
-
HT : High Voltage to the detector
-
Rad. det. : Signal to the detector
-
Signal out : Not used (amplified analog count signal)
-
Mains : Power input and primary power fuses (220 V: 1 A, 110 V :
2 A, slow blow)
-
F1 : Fuse 1A slow blow. For isolated +5V (Detector input, encoder
input, RS232 in/output)
-
F2 : Fuse 0.5 A slow blow. For detector HV.
-
F3 : Fuse 0.5 A slow blow. For isolated +/-15V (Detector input,
encoder input, RS232 output)
-
F4 : Fuse 0.5 A slow blow. The same as F3.
-
1 : For optional analog rate meter.
This chapter contains only small parts or changes of the paper manual.
-
Yearly maintenance is strongly advised for a long life time of accurate
working. This can only be done by a service technician.
-
Tools
-
X-ray optics alignment with a sealed tube
-
Detector HV adjustment
-
Encoders
-
Effic to check the X-ray/alignment efficiency:
the same as MACH3.
The values are the same. It needs a standard absorber, mounted on the collimator:
for Mo part number 0540.331, for Cu part number 0540.330.
-
Open the goniometer
-
Lubricate:
-
for omega and theta worm axis Teflon oil is used. It has no part number.
Ask Delft.
-
for the gearing wheels cad4 mach3 and kappaccd triflon greas
Part number SAP 4020016
-
No parts number for the oil we have a little
-
Upgrade to Express or Linux software
-
+5V adjustment
-
Replacement
Tools
-
Test crystal Ammonium bitartate. Order number 0516351T. Large crystal,
oriented. a = 7.648, b=7.844, c=11.068 Angstrom
X-ray optics alignment
with a sealed tube
The alignment is the same as with the MACH3,
with the exception:
There are now standard
absorbers which makes it possible to check if the intensity is all
right with the
EFFIC
measurement.
Det. error : for small adjustments and only when really needed, adjust
the detector position with the three Allen screws on both sides of the
detector stand. Direction:
Detector HV adjustment
-
Measure the intensity of the primary beam (see
safety)
with the MACH3 standard absorber with Mo : 30 kV 10 mA or Cu : 20 kV 10
mA.
-
Set in the pocket terminal: WD = 1000, LL = 100, HV = low (with xxx
MOVE WD/LL/HV)
-
Raise the HV untill the intensity reaches a plateau (after the plateau
it raises again, but that is dark current).
-
Set LL = 400 and adjust the HV, so the intensity at LL = 400 is half the
intensity of the previous plateau.
-
Fine adjust the HV, so the intensity at LL = 400 is half the intensity
with LL = 10. Then the sensitivity peak is situated at 400.
-
Input HV and default LL and WD in GONCON (values
changed in the pocket terminal are not saved)
Encoder ADC
zero/max
-
Remove on the goniostat the largest brown plastic cover.
-
Disconnect the top connector.
-
On the pocket terminal: MOVE, SPEC, PHI. Then it should show: PCC ####
-
Look into the interface to the Encoder board: the right one of set of boards
on the left. At the bottom, in the middle of the board, there are two adjustments.
-
Connect according A and adjust with the upper adjustment the pocket terminal
between PCC0003 and PCC0004
-
Connect according B and adjust with the lower adjustment the pocket terminal
jumping between PCC7773 and PCC7774. When you don't reach this value:
-
Measure the voltage between 0 V and 10V. When it is 10V then probably the
ADC converter on the Encoder board is defect and a new board must be bought.
-

Encoder adjustment
Phi coarse, zero adjustment (small adjustment if TEST ALL shows
a drift)
-
(A change of Phi coarse zero position is uncommon. Normally it only happens
when someone really repositioned the encoder)
-
Pocket: 0, move, Phi
-
Check on the mechanical dial if it is really at zero position
-
Pocket: spec, Phi, C/F to read PC (= position phi coarse).
This should be zero +/- 4.
-
If higher then loosen the three screws of the encoder (see above, red,
needs a 90 screw driverº) en rotate the coarse encoder till 0 +/-
2.
Open the
goniometer
-
Open
-
Remove the side plates of the indicators.
-
Remove two screws in the indicator with an long Allen key
-
Remove the cover and mount the indicator again (temporary with one screw)
prevent loosing the zero position of the indicators.
-
Close
-
Remove the indicators
-
Mount the enclosure
-
Position on zero
-
Mount the indicators in position zero.
Omega
cable change
Change of a cable running inside the omega axis for Phi and Kappa. This
can only be done with a new or a revised old CAD4. The holes of an old
CAD4 are too small to mount a new cable. Dismount the microscope support
and you will see the cables:
Change of the Phi cable:
-
Open the goniometer
-
Position Kappa on zero.
-
Remove the brown plastic cap from Phi.
-
Disconnect the plug (notice the colours) and dismount the Phi unit.
-
Remove the brass ring by rotating with a pointed pliers.
-
Remove the indicating wheel.
-
Remove the cable in the groove (encoder is the left cable) and mount the
new one. It should be glued deep in the groove, so it does not touch the
indicating wheel.
-
Pull the new cable trough the hole, trough the centre of the goniometer
to the bottom, and again trough a hole in the base upwards.
-
Solder the cable to the connector or cut the old cable some distance from
the connector and solder to the new cable.
-
When remounting, position the indicating wheel exactly on zero.
Phi unit (dis)mount
For returning the Phi encoder/motor unit for repair it must be remounted:
-
Dismounting
-
Position to zero.
-
Remove the largest brown cap (4 screws).
-
Disconnect the connector and remove the adhesive tape from the cable (make
a drawing how it is fastened, because the cable must be taped again in
the same way after remounting)
-
Remove three small screws close to the poles:
-

-
Slide the unit backwards.
-
Mounting
-
Position the Phi axis with the indicator to position zero and fix it with
tape.
-
Connect the flat cable to the Phi unit.
-
In pocket terminal: SPEC PHI C/F C/F.
This shows the course potmeter (PC) and fine potmeter (PF).
-
Adjust the Phi unit encoders till both readings are zero, first course
value then fine value.
-
Mount the phi unit in this position as shown above very careful so the
gears match. One can help this by rotating Phi slowly (> 2
MOVE PHI).
-
Fasten the Phi unit and position to zero (0 MOVE PHI).
You can try to position to exactly zero by rotating the Phi unit somewhat
when the screws are still loose, but it is not really needed because Phi
has a relative position which is anyway (the pin of the head) not exactly
zero.
Shutter dismount/remount
-
Can only be done by experienced service men.
-

-
Remove the monochromator.
-
Tube to zero degree (don't remove the tube holder).
-
Remove the sliding front plate (A). You will need a square screwdriver.
-
Mark the position of all parts, so you will remount it in exact the same
position. When remounting check all parts and rings, to remount it in the
same way.
-
Remove the filter disk. This must be done with two people. One keeps the
filter disk pressed against the holder, the other removes the screw in
the middle.
-
Tilt/remove the filter disk but be careful: behind the disk, on top, is
a spring with a steel ball which will jump away. So put some paper underneath.
-
Remove the shutter coil assembly with two screws right (B).
-
Remount all in the same position. When mounting the filter disk put some
grease in the hole and put the steel ball in, so it does not fall. The
spring remains in position.
-
Don't grease the shutter, because it needs special X-ray resistant grease.
Upgrade to
Express, Linux or PCDOS software
When upgrading to Express or Linux software and having a LSI
11 processor board (M7270), some changes must be made : See Product Change
Note 37 (ask Service).
When using VAX or PCDOS no change is needed.
With a Falcon (M8063) or Falcon+ (M7676) processor board no change is
needed.
+5V power adjustment
The +5V power supply is the large supply located in the left part of
the Interface behind the panel with the on/off switch.
-
Measure the +5V on the back of the Interface, on the computer backplane
(with the many pins), on the connector pins with the thick red and black
wire. It should above +4.8 V, also during start-up of the computer program
(when it draws a lot of current).
-
When it is much too low, the power supply is defect.
-
When it is a little too low you can adjust the power supply:
-
Remove all cables from the interface except the power cord.
-
Dismount the Interface and turn it up side down. You can reach a potmeter
on the power supply from the bottom.
-
Adjust the voltage carefully to 5.1V (not too high, because the electronics
is still connected).
Encoder
unit replacement
A single encoder can only be changed by an experienced servicemen.
A complete (encoder)unit is more easy to replace, but still needs some
experience:
Theta, Omega, Kappa
-
Position the axis exactly on zero.
-
Fix this position with tape, on the mechanical readers (Theta, Omega: remove
the side cover. Kappa: remove the brown plastic cover).
-
Switch off the electronics and solder the wires to the new encoder unit,
but do not yet mount it on the goniometer.
-
Switch on the electronics and readout both encoders in the pocket terminal:
spec, axis, C/F (C = course, F = fine)
-
Position the encoders with gear A on zero. First course, then fine.
-
Mount the encoder unit, with the screws fixed but not tight.
-
Check the backlash, by moving the internal gear B with a screw driver.
In fine reading it should change 1 bit. Not more, but also not less. Give
soft blows against the unit for small shifts in horizontal direction towards
or away from the axis gear C
-
Fasten the mounting screws
-
If the reading is no exactly zero in fine (mostly), then loosen the red
lacquered screws of the fine encoder and rotate the encoder a bit till
the reading is zero. Then fasten the screws.
-

Another, more complicated description can be found in an instruction
(1990, see PCN-list):
-
Kappa fine or coarse encoder.
-
Phi drive unit (includes motor and encoders)
-
Theta encoder unit.
| Program |
command |
file (n = default 0) |
PC-DOS
PC-LINUX
VMS - CAD4 |
GONCON, CASPAR or GCONST, O = output, M = modify, S = Save, Q = Quit,
I = input (asks to input all parameters) |
c : \CAD4\DATAn\ GONCAn.PAR
~/DATAn/ GONCAn.PAR (~ = login dir)
[CAD4.DATn] GONCAn.PAR |
| VMS - EXPRESS |
Goniometer constants |
[EXPRESS.DATAn] GONXAn.PAR |
GONCON, GCONST
| Command code |
Default |
|
| CON1 |
approx. 0.5868241 |
sin²(alpha) (Factory installed, alpha
= Kappa = approx. 50º) |
| CON2 |
approx. 0.6427876 |
cos(alpha) (Factory installed, alpha
= Kappa = approx. 50º) |
| CON3 |
approx. 0.0001787 |
cos²(89) * sin²(alpha) (Factory
installed, alpha = Kappa = approx. 50º) |
| THPOS |
77.50 |
Theta positive software limit in º |
| THNEG |
-49.00 |
Theta negative software limit in º |
| PDIST |
78.50 |
Distance crystal - Polaroid in mm |
| RADIUS |
173. |
Distance crystal - aperture/slits disk in mm |
| SLIT |
4.0 |
Manual horizontal slit in mm |
| APMAX |
5.9 |
Aperture vertical maximum in mm |
| APMIN |
1.3 |
Aperture vertical minimum in mm |
| MAXVAR |
xxxx |
Encoder position of maximum aperture |
| MINVAR |
xxxx |
Encoder position of minimum aperture |
| UPPERH |
xxxx |
Encoder position of upper hemisphere hole |
| LOWERH |
xxxx |
Encoder position of lower hemisphere hole |
| NEGSL |
xxxx |
Encoder position of skew slit, negative |
| POSSL |
xxxx |
Encoder position of skew slit, positive |
| VSLIT |
xxxx |
Encoder position of vertical slit |
| HSLIT |
xxxx |
Encoder position of horizontal slit |
| HOLE |
xxxx |
Encoder position of open hole |
| Attenuator filter factor and X-ray tube: see command WO
/ WI |
GONCON, CASPAR
| Command code |
Default |
|
| HV |
approx. 576 |
Detector high voltage in volt : see Adjustments |
| LL |
200 (Mo) or 100 (Cu) |
Detector low level |
| WD |
500 (Mo) or 600 (Cu) |
Detector window (LL + WD = max. 1275) |
| DT |
0.8300 |
Dead time in us |
| BR |
9600 |
CT port (Terminal) baudrate (not Host) |
| PA |
2. |
Axes positioning accuracy (in encoder digitization steps). A positioning
command only finishes when the end position (or end of a scan) is within
this value. |
| MT |
24 |
Motor gain for Theta |
| MP |
26 |
Motor gain for Phi |
| MO |
24 |
Motor gain for Omega |
| MK |
24 |
Motor gain for Kappa |
| MD |
24 |
Motor gain for Dial |
| FL |
NO |
Phi limit switch present |
| FL |
NO |
Special collar software present |
| FL |
NO |
Cryostat boundary software wanted |
| FL |
NO |
Turbo goniometer |
| FL |
NO |
Rotating anode. If NO: then a remote controlled HV generator is expected,
like the FR590. |
| EM |
60.0 |
HV generator emission trigger level in mA (normally not used) |
LED's
| Mains |
Run |
| +5V (digital) |
Indication of the halt switch (not indication of processor running) |
RS232 communication lines
| flash |
flash |
flash |
Flash when receiving data |
| PT |
CT |
CC |
|
| on |
flash |
flash |
Flash when transmitting data |
Pocket
terminal |
Terminal |
Host
computer |
|
Switches
| Mains |
Power |
| Run |
To stop/start the target program. Don't use this. Use mains to start-up.
Normal working position : down. |
| Angle, DX |
|
|
Mechanical readout |
|
|
|
|
coarse |
fine |
| Phi |
±180° |
|
360 °/rev, 2 °/div |
1 °/rev, 0.01 °/div |
|
|
±241° (for instance crystal oven) |
|
|
|
| Kappa |
±180° |
|
360 °/rev, 1 °/div |
1 °/rev, 0.01 °/div |
|
|
±60° (for instance helium cryostat) |
|
|
|
| Omega |
±250°, 0° is under the X-ray source |
|
counter, 1 °/step |
1 °/rev, 0.01 °/div |
| Theta, with sealed tube |
-50°, +77° , 0° is at the X-ray source |
|
counter, 1 °/step |
1 °/rev, 0.01 °/div |
|
|
|
|
|
| Speed |
Standard |
|
Turbo |
|
| Scan (Phi, Kappa, Omega, Theta) |
max. 16.5 °/min |
|
max. 16.5 °/min |
|
| Positioning |
max. 360 °/min |
|
max. 1000 °/min |
|
|
|
|
|
|
| Accuracy |
|
|
|
|
| Phi |
±0.015° |
|
|
|
| Kappa, Omega, 2Theta |
±0.010° |
|
|
|
| Reproducibility |
±0.0025° |
|
|
|
| Resolution |
0.0007° |
|
|
|
| Backlash, Phi, Kappa |
none |
|
|
|
|
|
0,007° |
|
|
|
|
|
0,0025° |
|
|
|
| Sphere of confusion |
R = 10 µm |
|
|
|
| -- |
|
|
|
|
| Microscope |
75 x, grid 0.036 mm/div, mounted on Omega +123° and +45° |
|
|
|
| Second microscope (option) |
125 x, mounted at +90 ° and 0 ° |
|
|
|
Anti-collision
-
Anti-collision software.
-
Axes maximum position switches. Turning back is possible.
-
Collision switches on both collimator holders.
X-ray optics
| X-ray source |
|
| Power |
maximum 60 kV, 300 mA |
| Crystal - focal point |
216.5 mm |
|
|
| Beta filters |
|
| Open hole |
beta/alpha = 13% |
| Cu |
0.020 mm nickel, beta/alpha = 0.2%, alpha transmission 42% |
| Mo |
0.108 mm zirconium, beta/alpha = 0.2%, alpha transmission 33% |
| Fe |
0.016 mm manganese, beta/alpha = 0.2%, alpha transmission 47% |
| - |
|
| Monochromator, sealed tube |
fine focus : Graphite, 12 x 6 mm, 0 0 2 reflection, mosaic spread approx.
0.4° |
| Collimators, sealed tube |
|
|
|
0.4 mm (1 ring), 0.8 mm (2 ring), 1.3 mm (3 ring) |
|
|
0.8 mm (1 ring), 1.3 mm (2 ring) |
|
|
| Dial, software control |
|
| 0,2 mm slits |
+45° (Pos), -45° (Neg), vertical, horizontal |
| 2 hemisphere |
horizontal |
| Aperture horizontal |
1.3 - 5.9 mm and open hole 9 mm. |
| Reproducibility slits |
±0.01 mm. |
| Crystal - slit |
173 mm |
| Aperture vertical (manual) |
1 mm, 2 mm, 3 mm, 4 mm, 6 mm. |
|
|
| Attenuator |
Cu : 0.06 mm Nickel, typical attenuation, 14x
Mo: 0.26 mm Zircon, typical attenuation, 14x |
| Beamstop |
Fine focus : 8 mm outside, inside Ø5.7 x 4 mm lead.
Normal focus : 12 mm outside, inside Ø9.1 x 4 mm lead. |
| Collimators detector |
2 mm, 5 mm. |
Detector
| Count rate |
<50 kcps |
| Accuracy |
<1% |
| Dark counts |
<0.1 cps |
| Scintillator |
NaI(T1) |
| Absorption |
Cu - Ag: 100% |
| HV adjustable |
-255 till -1020 V in 255 steps |
| Dead time |
Automatic compensation |
|
|
| Extension detector arm (option) |
Crystal - slit : 368 mm |
Goniometer heads
| Height |
49.0 mm |
| Distance ring |
14.96 mm |
| ECON head |
X, Y: ±1.5 mm Z: 8 mm |
| XYZ head (option) |
X, Y: ±2.5 mm Z: 8 mm |
| Eucentric head (option) |
X, Y: ±2.5 mm Z: 3 mm angle: ±15° |
The shutter does not open, or is closed when:
-
The collimator is not in the right position.
-
The monochromator or X-ray port is not in the right position.
-
The shutter-open lamps are defect.
-
The radiation enclosure is not closed.
-
When using a rotating anode: the goniometer is not properly placed in front
of the X-ray port.
The X-ray high voltage is not switched on, or is switched off when:
-
The shutter does not close.
-
The high voltage cable is not connected to the X-ray tube (indicated by
a link, attached to the cable and connected to the tube holder).
-
The X-ray on lamp is defect.
Safety override
The system is supplied with one override, which is only allowed to be
used during technical maintenance (see safety
rules).
-
Connecting a flashing Open-beam lamp to the enclosure connector on the
goniometer connector overrides the radiation enclosure safety. When the
lamp is defect the override is cancelled.
Safety with rotating anode generator FR591
With a X-ray generator all safeties are handled by the generator, except
the shutter safeties: collimator and beam stop.
Safety signals
-
Shutter-open lamp (red) : illuminated when the shutter is opened or is
not fully closed.
-
Shutter-closed lamp (green, only with sealed tube): illuminated when the
shutter is fully closed.
-
Open-beam lamp: flashes when the radiation enclosure safety is overridden.
-
X-ray lamp: illuminated when X-rays are generated.
With all lamps, excluded the green shutter-closed lamp, a defect lamp is
detected and activates the safety.
Safety with power off
Safety demands that circuits are automatically in a safe position when
they are out of order. So during power off, the goniometer Interface and
the X-ray high voltage are switched off by the safeties.
| Data line to Host |
RS232 : 50-38400 bd (the Interface determines with autobaud), 8 databits,
1 stop bit, odd parity. Hardware switchable to 20 mA loop. |
| Data line to pocket terminal |
RS232 : 1200 bd , 7 databits, 1 stop bit, no parity. (switch on with
CAPRT) |
| Data line to terminal/printer |
RS232 : 9600 bd (choice to 50 -38400 bd in CASPAR),
7 databits, 1 stop bit, odd parity.
A printer or terminal can be connected but also a PC with Windows can
act as a terminal with a terminal program which can be retrieved as a self
extractable file.
-
Extract the files in the directory you choose.
-
Start the program TERMINAL.EXE (windows program)
-
Load the settings with: File, Open, cad4-ct.trm
-
The default port is com 1. When you want to use another port, change
it in: Settings, communications (this setting can be file/saved).
|
| Crystal illumination |
Supply 24 V, max. 80 mA, 2 W. |
| X-ray / HV generator |
Hardware signals for shutter- and safety actions and a RS232 for software
communication. |
| Analog output |
Amplified analog counter signal. Ro = 50 Ohm |
| Rate meter |
Digital counter pulse and power supply for the Analog rate meter |
|
|
Programmable IC's
| Motor generator board |
IC25 |
600.25A |
For LSI-11 |
| 0546.600 |
|
MOT1B |
For Falcon and later. Can also be used in older equipment |
Radiation detection board.
0546.602 |
IC23 |
602.23A |
|
| Encoder readout board |
IC19 |
605.19A |
Probably for LSI11 |
| 0546.605 |
|
ENC3A |
For Falcon/Falcon+ |
|
IC5 |
605.05A |
For old version ADC |
|
|
ENC4A |
Last version from 1984 for new version ADC (PCN 26) |
|
IC6 |
605.06A |
For old version ADC |
|
|
ENC5A |
Last version from 1984 for new version ADC (PCN 26) |
| Personality module / QLC brd. |
IC1
IC2 |
606.01/2B
606.02B |
For LSI-11 (Does not work with DOS) |
| 0546.606/616 |
|
PMQ1C
PMQ2C |
For Falcon, with all software |
|
|
PMQ1E
PMQ2E |
For Falcon+, Falcon, with all software |
|
|
PMQ1F
PMQ2F |
For LSI-11, with DOS and VMS |
|
|
PMQ1G
PMQ2G |
For Falcon and Falcon+: newer 4 kB type. With hardware change (see
instruc. 15 May 1995) |
|
|
PMQ1H
PMQ2H |
For LSI-11: newer 4 kB. Needed for Linux/Express. This PROM is needed
when using Linux/Expres with hardware change (see PCN
37) |
|
IC3 |
606.03A |
For LSI-11 |
|
|
PMQ3B |
For Falcon |
|
IC4 |
606.04A |
For LSI-11 |
|
|
PMQ4A |
|
Radiation detection board
0546.612 |
IC1 |
RAD2A |
Can be used in all equipment |
| Bus Interface board |
IC4 |
BUS4A |
|
| 0546.604/614 |
IC12 |
604.12A |
For LSI-11 |
|
|
BUS1D |
For Falcon/Falcon+ |
|
IC40 |
606.40A |
|
|
|
BUS8A |
For new version 0546.614. Can also be used in older equipment |
|
IC42 |
BUS9A |
For Falcon/Falcon+ |
|
|
|
|
|
|
|
|